Persee Analytics Flame A3F (AAS) Atomic Absorption Spectrophotometer

Persee Analytics A3F Flame (AAS) Atomic Absorption Spectrophotometer

A3F – The instrument is equipped with a flame atomiser only. The positioning of which is fully controlled by the embedded computer system and AA-Win 3.0 software. Three flame options are available to the user with the Air/Acetylene being the standard configuration. This flame can be used for nearly all standard elements while the N2O/Acetylene and the Air/LPG (Natural gas) are available as an option for the more demanding elements. All three flame configurations offer coded burners for full safety protection.

Features
  • AAWin software
  • Light source
  • Background correction
  • Optical system
  • Autosampler

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The Persee Analytics A3F Flame (AAS) Atomic Absorption Spectrophotometer is equipped with a flame atomiser only. The positioning of which is fully controlled by the embedded computer system and AA-Win 3.0 software. Three flame options are available to the user with the Air/Acetylene being the standard configuration. This flame can be used for nearly all standard elements while the N2O/Acetylene and the Air/LPG (Natural gas) are available as an option for the more demanding elements. All three flame configurations offer coded burners for full safety protection.

Features

AAWin software

AAWin Software is a powerful and intuitive software product designed to allow control and data acquisition from the A3 series Atomic Absorption Spectrometer.
The AAWin software allows the Analyst to control all aspects of their analytical method whilst providing an extensive range of tools for data collection, storage, and interpretation.

Light source

Automatic 8 Hollow Cathode lamp turret controlled and optimized by the AAWin software. The operating lamp current and warm-up lamp current can be individually controlled to eliminate drift commonly associated with lamp warming.

Background correction

D2 lamp background correction system fitted as standard to all configurations. High-energy D2 lamps and adjustable beam splitter mirrors are optimized by the AA-Win software.

Self-Reversal background correction system fitted as standard to all configurations. The high-performance background system uses the same hollow cathode lamp as installed for the analysis. Minimum extra components are required and optical alignment is very simple. Self-reversal can be used for any element at any wavelength making it extremely versatile.

Optical system

High-precision minimal optics ensures maximum light throughput to the computer-controlled Czerny-Turner monochromator.

Autosampler

A universal autosampler is available as an optional accessory which is conveniently mounted on the front of the A3 instrument to automatically introduce standard and unknown samples to the atomizer for analysis.

Flame mode

The flame atomizer offers three flame options:

Air/Acetylene: The high sensitivity (Cu 2ppm >0.280abs) is due to the efficiency of the fixed-position glass nebulizer fitted as standard. An acid-resistant replacement is available as an option. The flame can be easily set from blue lean flame through stoichiometric to fuel rich by means of computer control.

N2O/Acetylene: This flame configuration is used to measure elements less prone to ionization such as: Aluminum, Tin, Titanium, Calcium, Vanadium and Molybdenum. Switching from Air/Acetylene to N2O/Acetylene to Flame Off is fully controlled by the AAWin3.0 software.

Air/Propane (LPG): Due to the Low temperature of the flame, it is ideal for analyzing alkali metals such as: Potassium, Sodium and Lithium, especially when used in the emission mode. Some remote areas of the world have difficulty obtaining Acetylene gas of a high enough purity to operate the flame correctly, LPG can give a real alternative and offer comparable results for most elements throughout the wavelength range.

Safety features
  • Pressure monitoring for all gases
  • Burner Identification
  • Flame sensor
  • Drain trap level sensor
  • Gas leak detector
  • Overpressure in premix
  • Safety cut-off switch
Principle

A3F is a highly sensitive analytical technique that can detect trace amounts of elements in a sample. The elements are heated and atomized in the pyrolytic graphite furnace, and become atomic vapour in the ground state, which selectively absorbs the characteristic radiation emitted by the hollow cathode lamp. Within a certain concentration range, its absorption intensity is proportional to the content of the element to be tested in the test solution.

Applications

A3G can be used for a wide range of applications including environmental science, agriculture, food science, pharmaceuticals etc.

Environmental science

A3G can be used to analyze soil, water, and air samples for heavy metals such as lead, mercury, and cadmium. This information is critical for understanding the impact of human activity on the environment and for monitoring compliance with environmental regulations.

Agriculture

A3G is used to analyze soil and plant tissues for the presence of essential elements such as nitrogen, phosphorus, and potassium. This information is important for optimizing crop yields and ensuring plants have the nutrients they need to grow.

Food science

A3G is used to analyze food samples for the presence of toxic elements such as arsenic and lead. This information is critical for ensuring that food products are safe for human consumption.

Pharmaceuticals

A3G is used to analyze drug formulations for the presence of impurities and contaminants. This information is important for ensuring that drugs are safe and effective for human use.

Specifications
Spectrometer System
Wavelength range 190-900 nm
Light source Hollow cathode lamp (HCL), Deuterium Arc lamp (D2)
Modulation Square wave pulse
Modulation frequency 100 hz self reversal (SR) background,
400 hz Deuterium Arc (D2) background
Monochromator 
Grating 1800 grooves/mm diffraction grating
Blazed wavelength 250 nm
Focus 300 nm
Bandwidth 0.1, 0.2, 0.5, 1.0, 2.0, 5.0 nm
Scan mode Automatic
Photometric type Single beam
Wavelength accuracy ±0.15 nm
Wavelength resolution 0.2 nm±0.02 nm
Wavelength reproducibility <0.05 nm
Spectral bandwidth 0.5, 1.0, 2.0, 5.0 nm
Baseline stability 0.005 A/30 min
Stray light ≤0.12 %T (220 nm NaI, 340 nm NaNO2)
Background correction Deuterium Arc (D2) 1.0 Abs,
Self Reversal (SR) 3.0 Abs
Flame Analysis
Flame types Air/Acetylene,
Nitrous Oxide/Acetylene,
Air/Propane (LPG)
Sensitivity (Cu) 2 μg/ml Absorption >0.280 Abs
Characteristic concentration Cu<0.02 μg/ml,
Ba<0.15 μg/ml (N2O/Acetylene)
Detection limit Cu<0.004 μg/ml
Repeatability Cu<0.7 % (Air/Acetylene Flame)
Ba<1.0 % (Nitrous Oxide/Acetylene Flame)
Burner heads Titanium alloy
Nebulizer High-efficiency glass,
Acid is available as an option
Pre-mix chamber Corrosion resistant
Atomizer selection Manual (A3F)
Automatic changeover (A3FG)
Safety features Burner identification, flame sensor, gas leak sensor, low gas pressure sensor, drain trap sensor, power loss protection
Graphite Furnace Analysis 
Graphite head Transversally heated
Temperature range Ambient-2650 ℃
Heating program Up to 10 steps. Drying, Ashing, Atomization, Cleaning
Feedback Voltage and optical temperature control feedback
Sensitivity (Cu) 50 ng/m Absorption>0.40 Abs
Detection limit  Cd<0.004 ng/ml
Repeatability Cu<2.0 %,
Cd<2.0 %
Graphite tubes Pyrolytically coated with platform
Sample size Up to 20μl
Safety features Burner Identification,
Flame Sensor,
Gas leak Sensor,
Low Gas Pressure Sensor,
Drain Trap Sensor,
Power Loss Protection,
Circulation Water (graphite),
Over Temperature Sensor (graphite)
Data Processing
Operating program AA Win Pro software
Analytical methods Flame AA, Flame AE,
Graphite Furnace,
Hydride Generation
Readout Mode Continuous, manual, peak height, peak area
calibrations Multi-standard calibration, standard addition, interpolation
Data storage Analytical results, instrument and measurement parameters, signal profile, calibration curve
Power Requirements
Main unit 220 VAC 50/60 Hz 200 W
Graphite power supply 380VAC 50/60Hz,
instantaneous power 5 kW current rating 7 kW
Dimensions 
Main unit 44 x 21 x 21 in
165 lb
Graphite power supply 20 x 21 x 21 in
154 lb

 

Catalog Number Model Number Description
A3F * 500F Flame (AAS) Atomic Absorption Spectrophotometer. A
data Data-coded air/Acetylene Burner is included
A3G 500G Graphite Furnace (GFAAS) Atomic Absorption
Spectrophotometer
A3FG 500FG Combined Flame & Graphite Furnace Atomic
Absorption Spectrophotometer. A Data Coded
An air/Acetylene Burner is included.

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